Organization
Support Laboratories

ICMM-CSIC

Nuclear Magnetic Resonance

 

Scientific Directors

Dr. Jesús Sanz Lázaro, Dra. Isabel Sobrados


Technician

Dra. Virginia Díez

 

Training Technician

Verónica López

 

Equipment

  • NMR Spectrometer AVANCE II (BRUKER), 9.4 Tesla magnet.
  • MAS probes for different spinning speeds for the study of a wide range of nuclei

 

 

Rotor

MAS spinning speed

Observed frequencies

2.5 mm

20 kHz

31P-15N (162-40.5 MHz)/1H-19F (400-376.5 MHz)

4 mm

10 kHz

31P-15N (162-40.5 MHz) /1H (400MHz)

4 mm

10 kHz

31P-13C (162-100 MHz) /19F (376.5 MHz)

7 mm

5 kHz

31P-13C (162-100 MHz) /1H (400MHz)

7 mm

5 kHz

13C-2H (100-61 MHz) /1H (400MHz)

7 mm

5 kHz

29Si-109Ag (79-18 MHz) /1H (400 MHz)

 

  • Static probe for pulse field gradient experiments (3 inserts available):
Tube diameter

Observed nucleus

temperature

5 mm

7Li

300-480 K

5 mm

1H

Room temperature

8 mm

7Li

Room temperature

  • Static probe for the study of single-crystal for nuclei 31P-109Ag (162-18 MHz).

 

Description

Its technical characteristics allow to perform several types of experiments:

  • Static experiments between -130 and 130ºC.
  • MAS experiments between -70 and 90ºC.
  • Decoupling experiments for proton and fluor.
  • CPMAS experiments with proton decoupling.
  • MQMAS experiments for quadrupolar nuclei.
  • Meassurements of diffusion coefficients.

Timetable

Mornings 09:00 - 14:00 Evenings: 15:00 -18:00

 

Telephone

+34 91 334 9000 ext. 553, +34 91 334 9075

Website

www.icmm.csic.es/nmr

 

e-mail

rmn@icmm.csic.es

 

Tariffs

  ICMM CSIC National Universities
and OPIS
Other

sample preparation and experimental start-up

2 € 3 € 3,5 € 7 €
hour** 14 € 25 € 30 € 60 €
night 84 € 150 € 180 € 360 €
weekend 168 € 300 € 360 € 720 €
report
ask for quotation
* These rates do not include taxes
** Minimum billing fraction: 0.5 hour

 

 

Application form   LIMS

 

 

       

ICMM-2017 - Sor Juana Inés de la Cruz, 3, Cantoblanco, 28049 Madrid, Spain. Tel: +34 91 334 9000. Fax: +34 91 372 0623. info@icmm.csic.es