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Home > Infrastructure > Support Laboratories |
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Scientific Director: Dra. María Dolores Serrano
Technicians: Maria del Carmen García González, Carolina Chaparro Ronda
Equipment:
- Atomic Absorption Spectrophotometre PERKIN ELMER mod. Analyst 300.
- Plasma Emission Spectrometre ICP PERKIN ELMER mod. OPTIMA 2100 DV
- CNHS Elemental Analyzer PERKIN ELMER 2400
Timetable: 09:00 - 15:00
Telephone: +34 91 334 9000 107-132-255
e-mail: mcarmengarcia@icmm.csic.es - carolina.chaparro@icmm.csic.es
Tariffs:
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ICP |
CHNS Analyzer |
ICMM / CSIC |
20 € / element |
8,5 € / sample
8
€ / > 8 samples |
Universities
and OPIS |
23 € / element |
10,5 € / sample
10
€ / > 8 samples
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Companies |
40 € / element |
20 € / sample
18,8
€ / > 8 samples |
For ICP if the number of samples of the same element is of:
- 1 - 5 samples 5 € / sample
- 6-10 samples 4 € / sample
- > 10 samples 3 € / sample
If the measurement time requires extra time the fee will be:
7 € / sample and element.
ICP application form: Solicitud.doc
CNH application form: Solicitud.doc |
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Scientists in charge: Prof. M. Lourdes Calzada; Prof. A. de Andrés; Dr. Álvaro Blanco
Technicians: 1 JAE-Tec
Equipments:
- Metal and graphite evaporator.
- Magnetron sputtering
- Plasma etching
- Spin coater
- Four-glove dry box (humidity and oxygen controlled down to 1ppm).
- Spin coater integrated.
- Flowlan for chemicals manipulation UV photolithography (available at the end of 2012)
Description: Clean room (class 10000) with a photolithography area (class 100)
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Scientific Directors: Dr. Enrique Chacón, Dr. Rafael Ramírez, Dr. Pedro Serena
Technicians: José Luis Amat
Web page |
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Scientific Director: Dr. Carlos Pecharromán García
Technicians: Rebeca Amaro Esteban, Pedro Rodríguez-Pascual
Equipments:
- 2 IR Spectrophotometres are availables:
- Nicolet FT-IR 20SXC (4000-400 cm-1)
- Bruker IFS 66V-S (10.000-50 cm-1)
With them we can analyze solid, powder, and liquid samples by transmission and refexion ( mirror, difuse, and weakend) in dry air, nitrogen, and vacuum atmosphere.
The spectral range goes from the far infra red (50 cm-1) upt to the visible (18.000 cm-1)
Description: The service processes the materials as received from the customer in order to prepare the samples for the IR spectrophotometres.
Timetable: 09:00 - 14:00
Telephone: +34 91 334 9000 ext. 161; +34 91 334 8991
e-mai: pmario@icmm.csic.es
Tariffs:
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€/Sample |
ICMM |
2,50 € |
CSIC |
3,50 € |
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€/hour |
Universities and OPIs |
15,00 € |
Companies |
40,00 € |
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Scientific Directors: Dr. Jesús Sanz Lázaro, Dra. Isabel Sobrados
Technician: Dra. Virginia Díez
Training Technician: Estefanía Toledano
Equipment: 
- NMR Spectrometer AVANCE II (BRUKER), 9.4 Tesla magnet.
- MAS probes for different spinning speeds for the study of a wide range of nuclei:
| Rotor |
MAS spinning speed |
Observed frequencies |
2.5 mm |
20 kHz |
31P-15N (162-40.5 MHz)/1H-19F (400-376.5 MHz) |
4 mm |
10 kHz |
31P-15N (162-40.5 MHz)/1H (400MHz) |
4 mm |
10 kHz |
31P-13C (162-100 MHz)/19F (376.5 MHz) |
7 mm |
5 kHz |
31P-13C (162-100 MHz)/1H (400MHz) |
7 mm |
5 kHz |
13C-2H (100-61 MHz)/1H (400MHz) |
7 mm |
5 kHz |
29Si-109Ag (79-18 MHz)/1H (400 MHz) |
- Static probe for pulse field gradient experiments (3 inserts available):
| Tube diameter |
Observed nucleus |
temperature |
5 mm |
7Li |
300-480 K |
5 mm |
1H |
Room temperature |
8 mm |
7Li |
Room temperature |
- Static probe for the study of single-crystal for nuclei 31P-109Ag (162-18 MHz).
Description: Its technical characteristics allow to perform several types of experiments:
- Static experiments between -130 and 130ºC.
- MAS experiments between -70 and 90ºC.
- Decoupling experiments for proton and fluor.
- CPMAS experiments with proton decoupling.
- MQMAS experiments for quadrupolar nuclei.
- Meassurements of diffusion coefficients.
Timetable: Mornings 09:00 - 14:00 Evenings: 15:00 -18:00
Telephone: +34 91 334 9000 ext. 553, +34 91 334 9075
e-mail: rmn@icmm.csic.es
Tariffs:
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Machine time
(spectra acquisition) €/h. |
ICMM |
14,00 € |
Universities and OPIs |
25,00 € |
Companies |
56,00 € |
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Scientific Director:
Dra. Elisa Román
Technician:
Adelaida Cintas
Equipments: Malvern Microslice 2 Cutter. Precision polish thinnig Logitech LP40.
Description:The techniques can be grouped in three categories:
- Single crystal cutting with disk diamond saw or poliurethane with incorporated goniometre.
- Single crystal orientations by X-ray Laue diagrams (with a precision of 0,5 degrees).
- Single crystal polish until optical finish.
Timetable: 08:00 - 14:00
Telephone: +34-91 334 9000 ext. 141, 132, 364
e-mail: acintas@icmm.csic.es
Tariffs:
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Sample cut
(up to 3 films) |
ICMM |
6,00 € |
Universities and OPIs |
12,00 € |
Companies |
18,00 € |
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Sample polish
(30 minutes grinder
and 1 hour polish) |
ICMM |
20,00 € |
Universities and OPIs |
40,00 € |
Companies |
60,00 € |
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Scientific Director: Dra. Agustina Asenjo
Website: http://www.icmm.csic.es/spm/
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Scientific Directors: : Dr. Eduardo Ruiz-Hitzky, Dr. Miguel A. Camblor, Javier Pérez-Carvajal 
Technician: Tomás García Somolinos
Equipment: The texture ananlysis laboratory has the following eqipment: Micrometritics ASAP 2010, Coulter Omnisorp 100 y Micromeritics Flowsorb 2300, for gas adsorptions and vapors on solids, and the recently acquired Poremaster Series Quantachrome Instruments for porosimetry measurement by Mercury intrusion on porous solids.
Description: The textural standard sample analysis is performed by N2 adsorption at 77 K.
- a. Single Point method.
- b. By analysis of the zone of relative pressures up to 0.35 and application of the BET method to the results.
- c. By analyzing micro and mesoporosity through the N2 adsorption-desorption isotherm.
Timetable: 09:00 - 14:00
Telephone: 91 334 9000 x 513, 126, 124, 159
e-mail: jperez@icmm.csic.es
Application form for textural characterization: solicitud fichero rtf
Contact person: Javier Pérez Carvajal
Tariffs:
Prices Euro/sample |
Techniques |
CSIC and UAM |
OPIS |
Companies |
Specific Surface BET
“1 point” |
20 € |
30 € |
45 € |
ASAP billed by the hours
Specific Surface BET multipoint: |
30 € |
40 € |
65 € |
Adsorption/Desorption isotherm |
80 € |
100 € |
150 € |
Microporosity with isotherm |
50 € |
80 € |
160 € |
| 24 hours |
150 € |
170 € |
250 € |
| longer than 24 h. |
2 € / additional hour |
Porosimeter |
70 € |
90 € |
190 € |
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Scientific Director :Dra. María Dolores Serrano
Technicians: Maria del Carmen García González, Carolina Chaparro Ronda
Equipment:
- Quadrupolar mass spectrometre for gas analysis, model THERMOSTAR QMS200 M3.
- Scanning differential calorimetry SEIKO
model DSC 220U; range temperature: -120 º C, + 700 º C.
- Simultaneous Differential Thermal Analysis / Thermogravimetric
SEIKO model EXSTAR 6300; range temperature: R. T. / 1000 º C.
- Simultaneous Thermal Analysis ATD/DSC/TG model Q600 TA Instruments; range temperature: R. T. / 1200 º C
Timetable: 09:30 - 14:00
Telephone: 913349000 ext. 107-132-255
e-mail: mcarmengarcia@icmm.csic.es - carolina.chaparro@icmm.csic.es
Tariffs:
Thermograms ATD/TG, DSC |
€ |
CSIC |
16,00 € |
Universities |
30,00 € |
OPIs |
30,00 € |
Companies |
68,00 € |
Mass Sspectrometría de Masas coupled to ATD/TG |
€ |
CSIC |
25,00 € |
Universities |
35,00 € |
OPIs |
35,00 € |
Companies |
78,00 € |
For DSC analysis requiring liquid N2 an extra fee of 20,00 € per
thermogram is charged. All prices are incremented an 18% VAT. |
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Application form for ATD-TG: Solicitud.rtf |
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Scientific Director:
Dra. Pilar Herrero
Technicians: Javier Ibarra, Francisca Ocaña
Web page: http://www.icmm.csic.es/tem/ |
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Scientific Coordinator: Dr. Enrique Gutiérrez Puebla
Scientific Director Powder Diffraction: Dra. Manuela Eloísa Medina Muñoz
Scientific Director Texture Analysis and Thin Fims: Dra. Ana Ruiz de Gopegui
Technician: José Berjano Larrea
Equipment:
- Powder Diffractometre Bruker D8 Advance with Cu Kα radiation with rapid detector (lynxeye).
- Powder Diffractometre Bruker D8 Advance with Cu Kα radiation with energy-discriminator (solx).
- Powder Diffractometre Panalytical X’pert with radiation of Cu Kα1.
- Texture AnalysisDiffractometre Bruker D8 Advance with Cu Kα radiation.
The equipments are homologated and controlled by the Nuclear National Security Board.
Description: X- ray powder diffraction diagrams.
Timetable: 09:00 - 15:00
Telephone: + 34 91 334 9000 ext. 021
e-mail: rx@icmm.csic.es
Tariffs: Tariffs 2010 |
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